土壤中 16 种 PAHs 提取技术的现状研究
摘要
萃取法、超声萃取法、QuEChERS、液相微萃取法、微波萃取法、超临界流体萃取法、固相微萃取法在实际土壤样
品中的应用情况及其优缺点。
关键词
全文:
PDF参考
[1] 土壤和沉积物多环芳烃的测定[M].高效液相色谱法,2016(5).
[2] 土壤和沉积物有机物分析方法第3部分:16种多环芳烃的测定气
相色谱—质谱法[Z].2022.
[3] 土壤和沉积物多环芳烃的测定气相色谱—质谱法[Z].2016.
[4] 李盛安.全自动索氏提取—气相色谱三重四极杆串联质谱法测
定土壤中18种多环芳烃[J].绿色科技,2018(22):23-26.
[5] 李莉.改进索氏提取器提取土壤中多环芳烃(菲、蒽、屈)[J].广
东化工,2011,38(3):143-145.
[6] 葛成军.土壤中多环芳烃不同前处理分析方法的比较[J].农业环
境科学学报,2009,28(4):859-864.
[7] Hawthorne. Comparisons of Soxhlet extraction, pressurized
liquid extraction, supercritical fluid extraction and subcritical
water extraction for environmental solids: recovery, selectivity
and effects on sample matrix[J]. Journal of Chromatography A,
2000,892(1):421-433.
[8] Graham, M.C. Investigation of extraction and clean-up procedures
used in the quantification and stable isotopic characterisation
环境与发展 5 卷 12 期 ISSN:2661-3735(Print);2661-3743(Online)
241
of PAHs in contaminated urban soils[J].Science of The Total
Environment,2006,360(1):81-89.
[9] 牟世芬.加速溶剂萃取的原理及应用[J].环境化学, 2001(3): p.
299-300.
[10] 张亚楠.加速溶剂-固相萃取-高效液相色谱法测定土壤及蚯蚓样
品中多环芳烃[J].分析化学,2016,44(10):1514-1520.
[11] 王娟.ASE-HPLC测定土壤中多环芳烃的方法研究[J].嘉兴学院
学报,2009,21(6):5-9.
[12] 许成君.快速溶剂萃取-水浴氮吹-高效液相色谱法检测土壤16种
多环芳烃[J].油气田环境保护,2022,32(2):49-55.
[13] 梁柱,余雯静,孙欣阳.加速溶剂萃取-色谱质谱联用法测定土壤
中的多环芳烃[J].化学分析计量,2009,18(3):45-48.
[14] 沈莹,朱月芳,孙欣阳.加速溶剂萃取—串联色谱质谱联用法测定
土壤中的多环芳烃[J].宁夏农林科技,2018,59(6):29-32.
[15] Wang, W. Extraction of polycyclic aromatic hydrocarbons and
organochlorine pesticides from soils: a comparison between Soxhlet
extraction, microwave-assisted extraction and accelerated solvent
extraction techniques[J]. Analytica chimica acta,2007,602(2):211-
222.
[16] 李兵.加速溶剂萃取技术在多环芳烃提取及检测中的应用[J].广
东化工,2012,39(1):55-56.
[17] 刘畅.土壤中多环芳烃不同提取技术评定[J].现代农业科
技,2012(18):216-217+225.
[18] Song, Y.F. Comparative study of extraction methods for the
determination of PAHs from contaminated soils and sediments[J].
Chemosphere,2002,48(9):993-1001.
[19] Heemken, O.P., N. Theobald, B.W. Wenclawiak, Comparison
of ASE and SFE with Soxhlet, Sonication, and Methanolic
Saponification Extractions for the Determination of Organic
Micropollutants in Marine Particulate Matter[J]. Analytical
Chemistry, 1997,69(11):2171-2180.
[20] Banjoo, D.R. P.K. Nelson, Improved ultrasonic extraction
p rocedu re fo r the dete rmination o f polycyclic a romatic
hydrocarbons in sediments[J]. Journal of Chromatography A,
2005,1066(1):9-18.
[21] 邹世春.超声—微波协同萃取装置用于土壤中多环芳烃的分析
[J].分析化学,2006(6):889-893.
[22] Yamaguchi, C. W.-Y. Lee, A cost effective, sensitive, and
environmentally friendly sample preparation method for
determination of polycyclic aromatic hydrocarbons in solid
samples[J]. Journal of Chromatography A, 2010,1217(44):6816-
6823.
[23] Stephens Jr, D.L. The effect of sonication on the recovery of
polycyclic aromatic hydrocarbons from coal stack ash surfaces[J].
Chemosphere,1994,28(10):1741-1747.
[24] 殷瑞君,王云平.土壤中PAHs提取纯化和测定方法研究进展[J].
山西农业科学,2017,45(11):1894-1899.
[25] 赵洁.改进QuEChERS-气相色谱—质谱法快速分析测定农用土
壤中多环芳烃[J].分析试验室,2012,31(2):33-37.
[26] Cvetkovic, J.S. Optimization of the QuEChERS extraction
p rocedu re fo r the dete rmination o f polycyclic a romatic
hydrocarbons in soil by gas chromatography-mass spectrometry[J].
Analytical Methods, 2016. 8(7):1711-1720.
[27] 杨维英.QuEChERs方法用于土壤中多环芳烃的应急监测研究
[J].农业与技术,2022.42(3):96-98.
[28] 吕爱娟.QuEChERS-高效液相色谱法快速测定稻谷和土壤中16
种多环芳烃[J].理化检验:化学分册,2016,52(9):1017-1021.
[29] 何成军, et al., QuEChERS-GC-MS/MS法快速测定地黄中12种多
环芳烃[J].中成药, 2023. 45(11): p. 3834-3839.
[30] 马晶,孙媛,康鹏.GC-MS/MS结合QuEChERS法测定土壤中16种
多环芳烃的方法研究[J].宁夏农林科技,2019,60(2): 1-3+18.
[31] 谭华东,张汇杰,武春媛.GC-MS结合微量QuEChERS法快速测定
土壤中16种多环芳烃[J].中国测试,2020,46(1):64-70.
[32] 王传咪.QuEChERS-分散液液微萃取结合GC-MS测定土壤中的
多环芳烃残留[J].化学试剂,2022,44(5):755-761.
[33] 朱会军,李菁华.QuEChERS方法在环境监测分析中的应用[J].化
工管理,2021(33):142-143.
[34] Jeannot, M.A. F.F. Cantwell, Solvent Microextraction into a Single
Drop[J]. Analytical Chemistry,1996,68(13):2236-2240.
[35] Rezaee, M. Determination of organic compounds in water
using dispersive liquid–liquid microextraction[J]. Journal of
Chromatography a, 2006,1116(2):1-9.
[36] 叶朝霞.分散液相微萃取-高效液相色谱法测定水和土壤中多环
芳烃[J].理化检验(化学分册),2012,48(4):467-470.
[37] Yazdanfar, N., et al., A Highly Sensitive Dispersive Microextraction
Method with Magnetic Carbon Nanocomposites Coupled with
Dispersive Liquid–Liquid Microextraction and Two Miscible
Stripping Solvents Followed by GC–MS for Quantification
of 16 PAHs in Environmental Samples[J]. Chromatographia,
2018,81(3):487-499.
[38] Jiang, X. and H.K. Lee, Solvent Bar Microextraction[J]. Analytical
Chemistry, 2004,76(18):5591-5596.
[39] Guo, L. H.K. Lee. Microwave assisted extraction combined
with solvent bar microextraction for one-step solvent-minimized
extraction, cleanup and preconcentration of polycyclic aromatic
hydrocarbons in soil samples[J]. Journal of Chromatography
A,2013(1286):9-15.
[40] 杨杰.微波萃取-高效液相色谱(HPLC)法测定土壤中16种多环芳
烃的研究[J].干旱环境监测,2006,20(1):5-7.
[41] 徐晖.微波辅助萃取-高效液相色谱法测定土壤中多环芳烃[J].华
中师范大学学报:自然科学版,2008,42(4):565-568.
[42] 林琳.微波提取高效液相色谱法测定土壤中15种痕量多环芳烃
环境与发展 5 卷 12 期 ISSN:2661-3735(Print);2661-3743(Online)
242
[J].中国环境监测,2009,25(2):86-89.
[43] 张玲金.固体模拟样品中多环芳烃有机污染物提取方法研究
[J].2003.
[44] Lutermann, C., et al., Effects of various binary and ternary
supercritical phases on the extraction of polycyclic aromatic
hydrocarbons from contaminated soils1Presented at the 2nd SFE,
SFC and XSE Symposium, Siegen, 8—9 October 1997.1[J].
Journal of Chromatography A, 1998,816(2):201-211.
[45] Hollender, J., et al., Efficiency of Different Methods and Solvents
for the Extraction of Polycyclic Aromatic Hydrocarbons from
Soils[J]. International Journal of Environmental Analytical
Chemistry, 2003,83(1):21-32.
[46] Librando, V. Supercritical fluid extraction of polycyclic aromatic
hydrocarbons from marine sediments and soil samples[J].
Chemosphere, 2004,54(8):1189-1197.
[47] Langenfeld, J.J. Role of modifiers for analytical-scale supercritical
fluid extraction of environmental samples[J]. Analytical
Chemistry,1994,66(6):909-916.
[48] Chiu, K.-H.Dry ice-originated supercritical and liquid carbon
dioxide extraction of organic pollutants from environmental
samples[J]. Talanta, 2005,65(1):149-154.
[49] Wicker, A.P., et al. On-line supercritical fluid extraction—
supercritical fluid chromatography-mass spectrometry of polycyclic
aromatic hydrocarbons in soil[J]. Journal of Chromatography B,
2018(1086):82-88.
[50] Ye, C.-W. Development and application of an SPME/GC method
for the determination of trace phthalates in beer using a calix[6]
arene fiber[J]. Analytica Chimica Acta,2009,641(1):64-74.
[51] Li, X., S. Gong, Z. Zeng, Development of a Sol-Gel Procedure
for Preparation of a Diglycidyloxycalix[4]arene Solid-Phase
Microextraction Fiber with Enhanced Extraction Efficiency[J].
Chromatographia, 2005,62(9):519-525.
[52] 张廉奉.三甲基杯[6]芳烃固相微萃取-气相色谱法测定土壤中的
多环芳烃[J].分析化学,2007,35(9):1269-1273.
[53] Fan, J. Monolithic graphene fibers for solid-phase microextraction[J].
Journal of Chromatography A, 2013(1320):27-32.
[54] Zhang, S., Z. Du, G. Li, Layer-by-Layer Fabrication of ChemicalBonded Graphene Coating for Solid-Phase Microextraction[J].
Analytical Chemistry, 2011,83(19):7531-7541.
[55] Xu, L. H.K. Lee, Novel approach to microwave-assisted extraction
and micro-solid-phase extraction from soil using graphite fibers as
sorbent[J]. Journal of Chromatography A, 2008. 1192(2): p. 203-
207.
[56] Wang, Y., et al., Quantitative determination of 16 polycyclic
aromatic hydrocarbons in soil samples using solid-phase
microextraction[J]. Journal of Separation Science, 2009. 32(22):
3951-3957.
[57] Rocha, M.J., et al., Determination of polycyclic aromatic
hydrocarbons in coastal sediments from the Porto region (Portugal)
by microwave-assisted extraction, followed by SPME and GCMS[J]. Journal of chromatographic science, 2011,49(9):695-701.
[58] Yiantzi, E., N. Kalogerakis, E. Psillakis, Vacuum-assisted
headspace solid phase microextraction of polycyclic aromatic
hydrocarbons in solid samples[J]. Analytica Chimica Acta,2015
(890): 108-116.
[59] Martendal, E. Carasek, A new approach based on a combination of
direct and headspace cold-fiber solid-phase microextraction modes
in the same procedure for the determination of polycyclic aromatic
hydrocarbons and phthalate esters in soil samples[J]. Journal of
Chromatography A, 2011. 1218(13):1707-1714.
[60] Doong, R.-a., S.-m. Chang, Y.-c. Sun. Solid-phase microextraction
and headspace solid-phase microextraction for the determination
of high molecular-weight polycyclic aromatic hydrocarbons in
water and soil samples[J]. Journal of chromatographic science,
2000,38(12):528-534.
[61] Pino, V. Micellar microwave-assisted extraction combined with
solid-phase microextraction for the determination of polycyclic
aromatic hydrocarbons in a certified marine sediment[J]. Analytica
Chimica Acta,2003,477(1):81-91.
[62] 杨然存,张少文,孙雨安.溶胶—凝胶杂化整体柱修饰及在多环芳
烃检测中的应用[J].色谱,2015(5):455-460.
[63] Feng, J. Poly(ionic liquids)-coated stainless-steel wires packed
into a polyether ether ketone tube for in-tube solid-phase
microextraction[J]. Journal of Separation Science, 2017,40(24):
4773-4779.
[64] Krüger, O. Comparison of Stir Bar Sorptive Extraction (SBSE)
and Solid Phase Microextraction (SPME) for the Analysis of
Polycyclic Aromatic Hydrocarbons (PAH) in Complex Aqueous
Soil Leachates[J]. Water, Air, & Soil Pollution, 2015,226(12):397.
DOI: http://dx.doi.org/10.12361/2661-3743-05-12-150535
Refbacks
- 当前没有refback。